Lipitor statins side effectsTable 2. Pharmacology of acetylcholine-induced responses. The pan used as the reference and the one filled with the sample, each measuring run was preceded by a blank experiment with the same reference pan and the sample pan, with its lid, empty and unsealed. The results of the blank procedure were recorded. Thereafter, the final measuring run was carried out by applying the same experimental conditions adopted in the blank experiment with always the same reference crucible and with the sample holder pan filled with the system under test. The above procedure was of paramount importance in the evaluation of the glass transition parameters as well as in the analysis of c p function of temperature. Greater details about both the instrument and the measuring procedures adopted in the thermal analysis can be found in Refs. 14, 15 . The parameter dH dt, where H is the enthalpy, could be measured within the range of 17 mW, using the highest instrumental sensitivity. We recall that, for condensed systems at constant pressure, the heat change Q is equal to the enthalpy change H for any thermal transition. The enthalpy values H in J g, constant pressure, associated with the melting process of the o- and m-toluidine, were evaluated with the thermal rate of 2 K min, because with the latter thermal rate the base lines for the integration of the melting peaks of the two liquids, are much better defined than with the 10 K min rate. The melting temperatures were evaluated with the Onset method to detect the intersection point of the evaluated regression line with the experimentally recorded baseline as well as the tangent to the experimental curve inflection point. For the glass transition three temperatures were evaluated, namely, T 1 at the intersection of the regression line from the start with the inflection tangent of the glass transition ``step, '' T 2 at the point where the transition of the sample is 50% complete and T 3 at the intersection of the inflection tangent with the regression line after the transition itself. Regression lines were computed before and after the glass transition, each one over 45 measuring points seconds . The description in extenso of the thermal analysis of o-toluidine will be reported elsewhere. The trend of c p function of decreasing temperature at the glass transition, is reported in Fig. 2 for both o- and m-toluidine. The same analysis performed upon heating the vitrified samples gave substantially the same results but for a shift to slightly lower values of the glass transition temperatures. The glass transition parameters for both o- and m-toluidine are reported in Table I for the thermal rates of 2 and 10 K min, m-toluidine was used as reference system. For the sake of completeness, the enthalpy values associated with the melting of both samples were also calculated from the NSC spectra 14, 15 collected by heating samples with a thermal rate of 2 K min. The calculated values are: H 71.2 J g for o-toluidine and H 82.5 J g for m-toluidine. The melting temperatures were T m 249.5 K and 242.2 K, respectively. As often reported in literature, the temperature T 2 can be taken as the glass transition temperature. According to the present analysis we found a value of T g 189 K for o-toluidine and a value of T g 188 K for m-toluidine, in agreement with the literature value T g 187 K 4 . Indeed the thermodynamic behavior of these two isomers at the, for example, effects lawsuit lipitor side. 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